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The extracts were introduced into a solvent-assisted distillation unit to complete the phase separation of the volatile components under ultra-high vacuum (10-5 mbar), and the obtained fractions were dehydrated by anhydrous sodium sulfate, further concentrated to 1.5 mL by Vigreux fractionation unit (50 cm 1 cm) and filtered by microporous membrane, and then concentrated by nitrogen purge to 1 mL

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