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After pooling the fractions containing pure 3,4- cis -leucocyanidin ( 6 ), MOPSO was added to a final concentration of 10 mM, the pH was set to 6.2 using 5 N NaOH and the pooled fractions were rotary-evaporated to a concentration of 7 mM of 3,4- cis -leucocyanidin ( 6 ), quantified by HPLC-UV (280 nm) with an external calibration curve with 3,4- trans -leucocyanidin ( 14 )

Nuclei were stained with DAPI and anti- -H2AX antibody was used to mark double-strand breaks sites

Dyes (Cy5.5, Cy7.5, or Nile Red) and P4 (100 mg) were co-dissolved in 1 mL DMSO, and the solution were then slowly added dropwise to 10 mL of water